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<span class="breadcrumbs"> 您現在的位置：<a href="/">首頁</a> > <a href="http://www.worksbymichaellawrence.com/newslist/idqsxea/">聯系我們</a> </span> </div> <div class="article-body uk-container-center"> <h2 class="article-title">如何校準ORP測定 <span class="n-date">DATE: 2023-12-04 21:00:38</span></h2> <div class="article-content"> <p><h5>業界資訊</h5>您的何校位置 : 精科儀器 > 業界資訊 > 如何校準ORP測定 <h1>如何校準ORP測定</h1>時間 : 2021-10-22 13:58:33 閱讀 : 62 氧化還原緩沖液是用于校準<strong>ORP電極</strong>的現成標準溶液。雖然ORP測量電極是測定金屬電極，但其零點和斜率不會有很大變化，何校<strong></strong>但可以用緩沖液發現小故障，測定如電<p>極性表面被污染或參考電極的何校零點偏移。</p><p>ORP儀表用氧化還原緩沖溶液校準，測定氧化還原緩沖溶液是何校鐵/鐵的標準溶液，有時奎寧氫醌飽和的測定酸性至中性緩沖溶液可用于校準。表5列出了具有不同參比電極的何校常用緩沖溶液的ORP測量值。其中UA為測量(毫伏)，測定對應于由30摩爾/升KCl銀/氯化銀H2SO4、何校<strong></strong>磷酸鐵、測定硫酸亞鐵/Fe2(SO4)3組成的何校電極；英國是測量(毫伏)，以飽和汞/甘汞電極為參考。測定UH是何校以標準氫電極為參考的相應測量值(毫伏)。EN值范圍從200毫伏到600毫伏。在這些校準溶液中，氧化還原電位電極具有高交換電流密度，因此氧化還原電位響應快，重現性好。氧化還原電位與酸堿度電極的不同之處在于零值不變，特征曲線斜率不變。然而，ORP值在實際測量中有時不正確。氧化還原電位電極必須清洗和再生，因為電極表面經常被污染。氧化還原電位電極測量氧化還原電位值不會在校準緩沖溶液中產生誤差。如果產生誤差，它們將由參比電極或其隔膜的故障引起。因此，使用ORP標準緩沖溶液校準檢測ORP電極表面狀態是不合適的。一般來說，用標準ORP校準緩沖液校準測量時，只限于檢查<strong>ORP電極</strong>組件系統的簡單功能。如果氧化還原電位值超出允許范圍，可能的原因是:</p><p>(1)使用了錯誤的參考電解液；</p><p>(2)由于對地短路，參比電極減少(參比電極對地DC電阻至少為10M *)；</p><p>(3)參比電極膜被污染；</p><p>(4)ORP電極內部接觸不良。</p><p>在校準過程中，還應注意氧化還原緩沖液可以還原電極表面的任何氧化鉑膜，因此在用緩沖液檢查電極性能后，鉑電極不能立即浸入強氧化樣品溶液中。取而代之的是，應該選擇</p><p>用自來水清洗，然后放入待測樣品測量。此外，還應注意，當用氧化還原緩沖液檢查氧化還原電極的性能時，應在電極預處理之前進行。</p></p><p><br></p></div> <div class="uk-grid 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