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<span class="breadcrumbs"> 您現在的位置：<a href="/">首頁</a> > <a href="http://www.worksbymichaellawrence.com/product_list/products.html">產品展示</a> </span> </div> <div class="article-body uk-container-center"> <h2 class="article-title">在使用COD快速測定儀測定中應該注意哪些問題？ <span class="n-date">DATE: 2023-11-03 02:45:29</span></h2> <div class="article-content"> <p><h5>公司動態</h5>您的使用速測位置 : 精科儀器 > 公司動態 > 在使用COD快速測定儀測定中應該注意哪些問題？ <h1>在使用COD快速測定儀測定中應該注意哪些問題？</h1>時間 : 2021-10-22 14:47:06 閱讀 : 271 　　水樣的化學需氧量也將由樣品容器保存，水樣，定儀清洗樣品，測定<strong></strong>分析水樣，該注添加試劑訂單，意問試劑質量和數量，使用速測添加氧化劑濃度，定儀反應溶液酸度，測定加熱的該注影響溫度和時間，滴定等條件。意問<br />　　<br />　　1，使用速測收集廢水樣本<br />　　<br />　　采樣z好在玻璃容器中取樣。定儀如果使用塑料容器進行取樣，測定酸度為，該注的意問<strong></strong>酸性樣品過高，會增加COD值。有必要收集有代表性的水樣。要做到這一點，我們必須先了解生產過程并了解研討會的排放規則。為了保存水樣，采樣后應迅速分析一些揮發性或不穩定的水樣。如果不能及時分析，可用硫酸調節水樣或放入冰箱2至5天。<br />　　<br />　　2，器具清洗和清洗<br />　　<br />　　新購買的全玻璃設備通常含有一些必須清潔的還原物質（有機物）。根據愚人節可以使用特定的清潔方法來消除比色管清潔方法和使用期間的預防措施。<br />　　<br />　　3，分析水樣量<br />　　<br />　?。?）應采用代表性的分析水樣不同的廢水成分需要以不同的方式取樣不均勻的采樣將導致大的分析錯誤，可歸納如下：<br />　　<br />　　一般清除無沉淀物的水樣或含少量沉淀物的水樣，搖勻水樣，用20mL單線移液管吸收;<br />　　<br />　　對于含有大量無機沉淀物的水樣，讓沉淀物下沉，然后吸收透明液體進行分析;<br />　　<br />　　對于含有漂白油的廢水，不僅應該搖動，而且要快速取樣;應采用1/4來測量適量的水。<br />　　<img src="http://image.jkcod.net/storage/16168/article/20211022/20211022084957_70787.jpg" alt="COD快速測定儀" title=""><br />　?。?）有機廢水中COD含量差異很大，總結如下。<br />　　<br />　　對于未知水樣，2mL水樣+ 1mLK2Cr2O7 + 3mLH2SO4可用于觀察消化比色管中的顏色變化。如果溶液呈黃綠色，取2mL水樣進行分析;如果溶液為藍色，取10mL水樣并稀釋取2 mL至100 mL進行分析。如果可以確定水樣中COD的近似范圍，可以在以下范圍內對樣品進行取樣和分析： COD小于200mg/L，在COD低范圍分析中可以取2mL水樣; COD為200~1000mg/L，2mL水樣取COD高范圍分析; COD在1000~10000mg/L，取10mL水樣+ 90mL蒸餾水進行稀釋分析;然后進行2mL分析。<br />　　<br />　　4，濃硫酸的影響<br />　　<br />　　應使用實驗室分析純（AR）來制備試劑。酸度高時，濃硫酸對重鉻酸鉀分解的分析結果較高;如果酸度很小，有些物質不能完全氧化，分析結果也很差。<br />　　<br />　　5，并行采樣<br />　　<br />　　在相同條件下，應使用相同的水樣同時測量兩個平行樣品，結果的分析程度用相對偏差表示。<br />　　<br />　　6，標準解決方案<br />　　<br />　　可以同時分析純有機物制備溶液或其他標準樣品和水樣品，并將添加的有機物質的理論需氧量值與實際測量的COD值進行比較?？刂品秶鸀?5％~105％。標準解決方案可以掌握分析過程的準確性。它還可以檢查儀器是否清潔且試劑是否準確。z廣泛使用的是鄰苯二甲酸氫鉀和葡萄糖。<br /><br />? ? ? ? <br /></p><p><br></p></div> <div class="uk-grid uk-grid-collapse nextpage"> <div class="uk-width-medium-1-10"> </div> <div class="uk-width-medium-5-10"> <a href="http://www.worksbymichaellawrence.com/html/139c299858.html">重慶鈑金加工廠要求</a> </div> <div class="uk-width-medium-4-10"> <a href="http://www.worksbymichaellawrence.com/html/290c299707.html">簡要說明化學需氧量測定儀器的檢測技巧</a> </div> </div> </div> <div class="footer-container"> <div class="uk-container-center footer"> <div class="uk-grid"> <div class="uk-width-medium-3-5"> <div class="uk-grid uk-grid-small"> <div class="uk-width-medium-1-5 uk-width-small-1-3 uk-width-1-3"> <dl> <dt><a href="http://www.worksbymichaellawrence.com/product_list/products.html" title="產品服務" target="_self">產品服務</a></dt> <dd><a href="http://www.worksbymichaellawrence.com/product_list/products.html" title="產品展示" 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