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class="breadcrumbs"> 您現在的位置：<a href="/">首頁</a> > <a href="http://www.worksbymichaellawrence.com/newslist/idqsxea/">聯系我們</a> </span> </div> <div class="article-body uk-container-center"> <h2 class="article-title">用標準化學需氧量消化器檢測時應消除氯離子的干擾 <span class="n-date">DATE: 2023-11-03 02:47:24</span></h2> <div class="article-content"> <p><h5>業界資訊</h5>您的用標氧量應消位置 : 精科儀器 > 業界資訊 > 用標準化學需氧量消化器檢測時應消除氯離子的干擾 <h1>用標準化學需氧量消化器檢測時應消除氯離子的干擾</h1>時間 : 2021-10-22 11:24:06 閱讀 : 65 標準化學需氧量消化器采用數字設置，顯示加熱溫度，準化自動控制加熱溫度，學需消化<strong></strong>可設置加熱時間。器檢化學需氧量快速測定儀器是測時除氯一種基于催化法快速的實驗室精密分析儀器，采用單色冷光源測量有色溶液變色技術處理數據。干擾升溫快、用標氧量應消溫度恒定均勻、準化功耗低、學需消化<strong></strong>操作簡單、器檢性能穩定可靠，測時除氯廣泛應用于環保、干擾醫療、用標氧量應消衛生、準化食品、學需消化自來水、造紙、污水處理、印染、石化、金屬冶煉、高校等行業。在化學需氧量值為測定的過程中，樣品中的氯離子會干擾測定，使測定的結果與實際值相差很大。因此，在水樣被消化之前，必須消除氯離子的干擾。本方法使用一定量的硫(化學符號:S)酸汞作為掩蔽劑，可用于測定高氯水樣，無干擾。<p>測定標準化學需氧量消化池工藝:</p><p>1。分別吸取3毫升蒸餾水(空白)或混合均勻的水樣，并將其放入干凈的反應管中。氨氮測定儀采用標準:水楊酸比色法完成水質氨氮測量，采用國際標準規定的二氯異硫氰酸鈉代替常用次氯酸鈉，大大提高了試劑溶液的含氯穩定性和有效性(b型)</p><p>2。在每個反應管中加入1mL掩蔽劑，搖勻。</p><p>3、在每個反應管中加入1mL氧化劑(100-1200mg/L范圍)和5mL催化劑，用塞子搖勻?；瘜W需氧量檢測儀器的標準方法測定采用回流消解滴定法。該方法消化時間長(2小時)，能耗大，試劑成本高，效率低，經常困擾實際操作人員。</p><p>4。將反應管依次插入消化爐孔中，待降低溫度設定在165℃后進行加壓。消化；鍵，儀器設備自動定時消化，消化后蜂鳴器報警。</p><p>5。取出反應管試管架，自然冷卻2分鐘，然后冷卻至室溫。</p><p>6、擰開塞子，將反應管中的溶液倒入小三角瓶中，用少量水沖洗反應管和蓋子(滴定前的總體積為50毫升)，加入5mL濃H2SO4(分析純)，用水稀釋50毫升。</p><p>7。冷卻后，加入3滴亞鐵指示劑，用硫酸亞鐵銨標準滴定劑滴定溶液。滴定溶液的顏色從黃色變為紅棕色，直至藍綠色，這是終點。記錄硫酸亞鐵銨標準滴定溶液的消耗毫升V2。</p></p><p><br></p></div> <div class="uk-grid uk-grid-collapse nextpage"> <div 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